PSS offers pumping systems for all GPC/SEC needs, providing excellent flow and composition stability over a wide range of flow rate ranges. Hardware and software of all SECcurity GPC1260 pumps are designed for easy setup, operation, maintenance and early recognition of problems. All pumps and degassers can be used also with difficult GPC/SEC solvents including hexafluoroisopropanol HFIP.
| isocratic pump | P/N 404-0101 |
| binary pump | P/N 404-0102 |
| quaternary pump | P/N 404-0103 |
| vacuum degasser 2 channels | P/N 409-0024 |
| vacuum degasser 4 channels | P/N 409-0031 |
SECcurity isocratic pump
SECcurity 1260 isocratic pumpThe ideal GPC/SEC pump with highest run-to-run and day-to-day precision of retention times. The optimized design ensures virtually pulse-free and stable solvent flow, with dual floating pistons in series, precisely servo-controlled. This delivery principle allows variable stroke volume optimized to selected flow rate. An inlet-valve electronically activated and synchronized to piston stroke - eliminates vapor formation with volatile solvent. Low operating and maintenance costs - due to long instrument uptime. Versatile wide flow range - up to 10 mL/min, including semi-preparative separations. Robust materials withstand most demanding applications - stainless steel, titanium, gold, ruby, sapphire, ceramics, PEEK and PTFE ensure long lifetime. Seal wash option for high salt mobile phases keeps maintenance to a minimum for lower operation costs.
| Specifications | |
| Flow | |
| Precision | ≤0.07 % RSD,or ≤0.02 min SD whatever is greater, based on retention time at constant room temperature |
| Accuracy | ± 1 % or 10 µL/min whatever is greater |
| Range | Setpoints from 0.001 to 10.0 mL/min, in 0.001 mL/min increments |
| Pressure | |
| Operating range | 0 - 60 MPa (0 - 600 bar, 0 - 5880 psi) up to 5 mL/min 0 - 20 MPa (0 - 200 bar, 0 - 2950 psi) up to 10 mL/min |
| Pulsation | <2 % amplitude (typically <1 %) at 1 mL/min isopropanol at all pressures >1 MPa (> 10 bar, >147 psi) |
| Compress. compensation | User selectable, based on mobile phase compressibility |
| pH range | 1.0 - 12.5 Solvents with pH <2.3 should not contain acids which attack steel |
| GLP/Compliance | Electronic records of maintenance and errors. Early maintenance feedback (EMF) for continuous tracking of instrument usage, display of feedback messages if preset limits are exceeded. |
Part number: 404-0101
Option seal wash: 404-0116
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SECcurity binary pump
The SECcurity binary pump is based on a high-pressure mixing principle. It is the pump of choice for reproducible gradients and high performance, especially at low flow rates and for high throughput applications. It has an optional programmable solvent selection valve which combines two out of four solvents for utmost flexibility and increased convenience, for example, when flushing the column. The binary pump is also ideally suited to do standard-bore chromatography. Floating pistons with path-of-least-resistance principle ensures highest seal lifetime.
| Specifications | |
| Flow | |
| Precision | ≤0.07 % RSD,or ≤0.02 min SD whatever is greater, based on retention time at constant room temperature |
| Accuracy | ± 1 % or 10 µL/min whatever is greater |
| Range | Setpoints from 0.001 to 5.0 mL/min, in 0.001 mL/min increments |
| Pressure | |
| Operating range | 0 - 60 MPa (0 - 600 bar, 0 - 5880 psi) up to 5 mL/min |
| Pulsation | <5 % amplitude (typically <2 %) at 1 mL/min isopropanol at all pressures > 1 MPa (10 bar) |
| Compress. compensation | User selectable, based on mobile phase compressibility |
| Gradient | |
| Delay volume | Standard delay volume configuration: 600-800 µL, dependent on back pressure (includes 400 µL mixer) Low delay volume configuration: 120 µL |
| Composition precision | <0.15 % RSD, 1 mL/min |
| Composition accuracy | <0.35 % absolute |
| pH range | 1.0 - 12.5 Solvents with pH <2.3 should not contain acids which attack steel |
| GLP/Compliance | Electronic records of maintenance and errors. Early maintenance feedback (EMF) for continuous tracking of instrument usage, display of feedback messages if preset limits are exceeded. |
Part number: 404-0102
Option seal wash: 404-0124
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SECcurity quarternary pump
The SECcurity quaternary pump is a pump for low pressure mixing of up to four solvents. The quaternary pump provides highest flexibility in solvent mixing and is recommended for a wide range of research and routine applications, and in the method development area. It ensures virtually pulse-free and stable solvent flow, with dual floating pistons in series, precisely servo-controlled. The variable stroke volume allows pulse-free solvent delivery and efficient mixing. Keeps maintenance to a minimum for lower operation costs by using robust materials such as stainless steel, titanium, gold, ruby, sapphire, ceramics, PEEK and PTFE. Optional active seal wash option for high salt mobile phases to prevent corrosion. Wide flow range of up to 10 mL/min, including semi-preparative separations.
| Specifications | |
| Flow | |
| Precision | ≤0.07 % RSD,or ≤0.02 min SD whatever is greater, based on retention time at constant room temperature |
| Accuracy | ± 1 % or 10 µL/min whatever is greater |
| Range | Setpoints from 0.001 to 10.0 mL/min, in 0.001 mL/min increments |
| Pressure | |
| Operating range | 0 - 40 MPa (0 - 400 bar, 0 - 5880 psi) up to 5 mL/min |
| Pulsation | <2 % amplitude (typically <1.3 %) at 1 mL/min isopropanol at all pressures >1 MPa (> 10 bar, >147 psi) |
| Compress. compensation | User selectable, based on mobile phase compressibility |
| Gradient | |
| Delay volume | 800 - 1100 µL depending on back pressure |
| Composition precision | <0.20 % SD, at 0.2 and 1 mL/min |
| pH range | 1.0 - 12.5 Solvents with pH <2.3 should not contain acids which attack steel |
| GLP/Compliance | Electronic records of maintenance and errors. Early maintenance feedback (EMF) for continuous tracking of instrument usage, display of feedback messages if preset limits are exceeded. |
Part number: 404-0103
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SECcurity vacuum degasser
Special on-line vacuum degasser for all GPC/SEC eluents including hexafluoroisopropanol HFIP. The degasser has two, three, or four independent solvent channels with a small volume for optimum degassing up to a flowrate of 3 ml/min. The two (three) channel degasser is modular upgradable to add additional independent solvent channels.
| Specifications | |
| Number of Channels | 2, 3, 4 |
| Internal Channel Volume | 480 ml |
| wetted parts | PEEK, Teflon AF® |
| Life expectancy | 5 years continous run |
| GLP/Compliance | validation analog out 5 mVDC / 1 mm Hg ±1.0% |
Part numbers:
2 channel degasser: 409-0024
4 channel degasser: 409-0031
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