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PSS - Polmer Standards Service

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GPC/SEC Troubleshooting

GPC/SEC Troubleshooting has been developed by PSS and Separation Science. It is published bimonthly in ChromDoctor section of Separation Science Magazine since March 2010:

 

AuthorTitleQuestionSep.Sciencepdf
D. Held

#4

Unexpected peak shapes  – different shapes than others

I have measured calibration standards to create a calibration curve and they look different from the manufacturer

’s peaks. What is wrong?
magazine linkInfo
D. Held#3 Additional Gost or System PeaksI see a lot of peaks, especially in the low molar mass region of the chromatogram. Is that normal? magazine linkInfo
D. Held#2 Missing SignalI have injected a sample and I don't see a signal. What can be the reason for this?magazine linkInfo
D. Held#1 Pressure IncreaseMy GPC/SEC system runs at a pressure of 80 bar/1160 psi. Now the system pressure has been increased and the pump has shut down to protect the columns. What should I do?magazine linkInfo

 

 

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Polefin HT-GPC Columns

For HT-GPC separations, applicable wíth light scattering detectorsweiterlesen